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A Virtual Instrumental Analysis Laboratory (VIAL) A Virtual Instrumental Analysis Laboratory (VIAL)

A Virtual Instrumental Analysis Laboratory (VIAL) - PowerPoint Presentation

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A Virtual Instrumental Analysis Laboratory (VIAL) - PPT Presentation

for Buffalo State and Open SUNY Jinseok Heo Alexander Nazarenko M Scott Goodman and Jamie Kime Department of Chemistry Buffalo State College RESULTS CONCLUSIONS AND PLANS BACKGROUND INFORMATION ID: 807399

instruments analytical buffalo lab analytical instruments lab buffalo state campus tutorials analysis suny data video instrument skills students class

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Slide1

A Virtual Instrumental Analysis Laboratory (VIAL)

for Buffalo State and Open SUNY

Jinseok Heo, Alexander

Nazarenko

, M. Scott Goodman, and Jamie

KimeDepartment of Chemistry, Buffalo State College

RESULTS

CONCLUSIONS AND PLANS

BACKGROUND INFORMATION

ABSTRACT

We present the development of a Virtual Instrumental Analysis Laboratory (VIAL) platform for Buffalo State and SUNY campuses. We will report the effectiveness of the VIAL for students’ gaining knowledge and skills in using advanced analytical instruments that were newly acquired in the Department of Chemistry at Buffalo State College.We will also show the possibility of remote controlling of the analytical instruments, so that off-campus users can directly benefit from our advanced facilities.

PROPOSED IDEA

ACKNOWLEDGEMENTS

IITG 2013 GrantMegan Niesyty, Jennifer Gibson, and Anna Copelad (Buffalo State Students)

AIMS of the PROJECT

Aim 1. To effectively educate students to use modern analytical instruments by combining virtual and hands-on lab experiencesAim 2. To provide learning opportunities with advanced analytical instruments to students, faculty, and staff at other SUNY institutionsAim 3. To provide professional training on data acquisition and processing to the local scientific community (Future)Aim 4. To investigate the feasibility of remote control of advanced analytical instruments (Future)

What is Analytical Chemistry?

Quantitative

Analysis

Qualitative

Analysis

Wet analysis

Instrumental analysis

Skills and knowledge required for instrumental analysis

Knowledge of the principles and the hardware of the instrument

Reliable data

Troubleshooting for the instruments

Knowledge of the software for the instrument

Collect, process, and analyze data

Skills of using software package for plotting graphs and treating data statistically

Present data

Acquisition of major analytical instruments

with the opening of new science building

at Buffalo State in Spring 2013

Buffalo State Campus

Students

O

n-site education and training?

Other SUNY

Campus

OPEN SUNY?

WNY community

Service?

On-line tutorials on analytical instruments (AIMS 1 & 2)

Include

descriptions of the underlying principles of the analysis, sample preparation steps, instructions on the software for acquiring and processing data, demonstrations of running the instruments, and simple maintenance procedures

.

Use animation, video clips, on-line test, and webinar

Available through Blackboard and eventually available through SUNY digital repository

Buffalo State CHE 403 course materials posted in Blackboard (Spring 2014)

Live demonstrations of the equipment with audio, video,

and screen-sharing tools (AIMS 1 - 3)

Include live demo and recording for later viewing on campus

Can be extended to off-campus scientific community in future

Remote control of analytical instruments (AIM 4)

Buffalo State Campus

Other SUNY

Campus

Instrument A

User

Lab Manager

Control

Data

Sample

Creation of video tutorials on analytical instruments

Four faculty experts participated in this project

Dr. Jinseok Heo for Thermo DXR Raman microscope (5 tutorials)

Dr. Jamie Kim for Agilent GC and GC-MS and Shimadzu GC (3 tutorials)

Dr. Scott Goodman for

Bruker

Avance

III NMR (in-progress)

Dr.

Alexandaer

Nazarenko

for

Bruker

D8 Venture X-ray

diffractometer

(in-progress)

Video tutorials created by Heo and his student

Assessment of the effect of video tutorials on students’ skills on analytical instrument

Assessed 11 students enrolled in CHE 403 (analytical instrument) class of Spring 2014Two analytical instruments were chosen. One lab experiment (Raman lab) was provided with video tutorials but the other lab (IR lab) was with a conventional lab manual format.Compared the class average scores of the two lab reports At the end of the semester students’ performing skills on the two instruments were assessed and the class averages for the two instruments were compared. We did not find any statistical difference between the Raman lab and the IR lab from the perspective of lab report scores and practical lab skills. Managing the analytical lab was much easier after introducing the video tutorials. Interacting with broader groups of students were made possible.

Live demonstration of analytical instrument using remote desktop connection

In-class demonstration of Ft-IR instrumentlocated in other lab.The instrument could be controlled by the in-class computer through remote desktopconnection.

VIAL

platform is potentially useful for helping students acquire skills

and knowledge required for analytical instruments but more data is needed

to make a decisive conclusion.

More video tutorials will be incorporated to assist lab courses at Buffalo

State and will be available through SUNY digital repository.

We demonstrate that analytical instruments can be remotely controlled

on-campus. Theoretically off-campus users may access to

them.