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1 	   SYED MUHAMMAD ALI NAQVI 1 	   SYED MUHAMMAD ALI NAQVI

1 SYED MUHAMMAD ALI NAQVI - PowerPoint Presentation

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1 SYED MUHAMMAD ALI NAQVI - PPT Presentation

Management Associate Presentation Presented by Losses Control at DAP PLANT 2 Purpose To reduce the losses and recover into system for optimizing Plant Process 3 Scope of Presentation ID: 568810

nm3 loss ammonia dust loss nm3 dust ammonia acid losses scrubber dryer stack operating reasons phosphoric dap comparison plant

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Presentation Transcript

Slide1

1Slide2

SYED MUHAMMAD ALI NAQVI

(Management Associate)

Presentation

Presented by:

Losses Control at DAP PLANT

2Slide3

Purpose

To reduce the losses and recover into system for optimizing Plant Process

3Slide4

Scope of Presentation

Reasons and Recovery of Ammonia Loss

Reasons, Effects and Recovery of Dust Loss

Losses Emission Points

Losses at DAP Plant

Background

Stack Losses and comparison of Design & Operating conditions

Suggestion

4Slide5

Background

In any Process industry, Loss of Nutrients (either from Raw material or Product) is the Loss of Money, Loss in Profit and mitigation of Production rate.

5Slide6

Losses at DAP Plant

Losses at DAP Plant

Dust Lost

Ammonia Loss

P

2

O

5

Loss

6Slide7

Recycle Belt Conveyor

Pre neutralizer

Granulator

Dryer

Primary Screens

Oversize Crusher

Product Conveyor

Polishing Screens

F.B.C

Gaseous Ammonia

Scrubbing Liquor

Phosphoric Acid

H

2

SO

4

Liquid Ammonia

GPR

Granulator feed bucket elevator

Primary Screen Feed Elevator

Dedustig

Section

Scrubbing Section

Dust Loss

Ammonia Loss

Stack

Chilled Air

Coater

Polishing screen feed elevator

Recycle Solids

Losses Emission Points

7Slide8

Reasons of Dust Loss

Reasons of

Dust

Loss

Quality of Phosphoric Acid

Limitation of Dedusting Section

8Slide9

Effect of Dust Emission

Continuous reclaiming of dust

Housekeeping

9Slide10

Hopper

Dryer

Dedust

Cyclone

Dryer Exhaust Fan

Dusty gases from Dryer

Dryer Venturi Scrubber

Recycle Belt (DM-223)

Dust

Dust Recovery

Hopper

Dedust

Cyclone

Dedusting Exhaust Fan

Dusty air from Conveyors, Elevators, Screens

Granulator

Bag house

Instrument Air

10Slide11

Reasons of Ammonia Loss

Reasons of

Ammonia Loss

Poor working of Scrubbing

Frequent Shutdown & startup

11Slide12

Schematic diagram for Ammonia Recovery

PRE-SCRUBBER

PN & Granulator Gases

RG SCRUBBER

TAIL GAS SCRUBBER

STACK

Dryer SCRUBBER

PRIMARY SCRUBBER TANK

Phosphoric Acid

Industrial Water

H

2

SO

4

PN Reactor

50-70 %NH

3

recovered

Above 90%NH

3

recovered

From Dryer exhaust fan

Above

95%NH

3

recovered

Maximum NH

3

recovered

Atmosphere

12Slide13

Stack losses

Component

Design Loss

Actual Loss in 2011

Actual loss during 2012Particulate matter150 mg/NM3

<10 mg/NM3

<10 mg/NM3

Ammonia100 mg/NM379 mg/NM373 mg/NM3P2O536

mg/NM

3

<10

mg/NM

3

<10

mg/NM

3

Fluoride

30

mg/NM3

<1 mg/NM3<1 mg/NM3

13Slide14

Suggestion

Good quality of Phosphoric acid should be used.

Size of flappers of Dedusting hoppers should be increased for increasing suction of Dedusting Fans for lowering emission of dust in operating area.

Scrapper system of Recycle belt (DM-223) should be maintained properly.Provision of Dual strainers in the discharge of RG scrubber Pump(DP-5012).14Slide15

Thank You

15Slide16

Comparison of Stack Dust Loss(mg/NM

3

) b/w Operating & Design conditions

16Slide17

Comparison of Stack Ammonia Loss(mg/NM

3

) b/w Operating and Design Conditions

17Slide18

Comparison of Stack P

2

O5 Loss(mg/NM3

) b/w Operating and Design Conditions

18Slide19

Dedust cyclones and Bag house Analysis

Equipment

Date

Component

UnitInlet DuctOutlet DuctDD-431

26/4/12Dust

g/NM3

9066DD-403226/4/12Dustg/NM3

408

4

DD-433

26/4/12

Dust

g/NM

3

322

8

Bag

House

26/4/12Dustg/NM3

5.04

19Slide20

Phosphoric Acid

SHIPMENTS

Composition: Range 111

th

112

th

113

th 114th

P2O5 52.00 – 54.00 54.2 53.4 53.1 53.3

Fe

2

O

3

0.40 – 1.00 0.39 0.43 0.41 0.45

Al

2

O

3

0.50 – 1.00 0.36 0.47 0.48 0.50

F 0.30 – 0.50 0.22 0.33 0.33 0.35

CaO

0.05 – 0.30 0.03 0.02 0.04 0.01

MgO

0.12 – 1.30 0.70 0.76 0.69 0.70

20Slide21

Analysis of three types of phosphoric acid produced by acidulation of different phosphate rocks

Item Acid A (wt%) Acid B (wt%) Acid C (wt%)

P

2O5 50.50 52.14 51.29

Fe2O3 1.250 0.580 0.120

Al2O3 0.981 0.714 0.200

F- 0.640 0.610 0.630

CaO 0.090 0.083 0.104MgO 0.610 0.570 0.552

21Slide22

Comparison of the effects of impurities on the number of

fine particles and granulation quality of produced

DAP

22Slide23

Operating Range of Scrubbing Section

23