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Advanced Materials Characterization Core Advanced Materials Characterization Core

Advanced Materials Characterization Core - PowerPoint Presentation

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Uploaded On 2024-03-13

Advanced Materials Characterization Core - PPT Presentation

Director Dr Paul A Baker Department of Physics CAS Contact emails pabakeruabedu vthomasuabedu charitauabedu Scanning Electron Microscope SEM ID: 1046901

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1. Advanced Materials Characterization CoreDirector: Dr. Paul A. Baker, Department of Physics, CAS. Contact emails: pabaker@uab.edu, vthomas@uab.edu, charita@uab.eduScanning Electron Microscope (SEM): Multi-Purpose X-ray Diffraction (XRD): Raman Spectroscopy X-ray Photoelectron Spectroscopy (XPS): Atomic Force Microscopy (AFM): AFM instrument and images of collagen nanomatrix and polymer spherullitesInfrared Spectroscopy (Micro-FTIR): Typical FT-IR spectra of polymer and proteinNano-indenter : Image after indentationOrthopedic and Dental Joints Wear Simulator:Materials Characterization Services:Image nanocale surface features and morphologies of metals, biomaterials, thin films, particles, polymers, proteins and other biometrices, grain boundaries, composites etc.Two AFM instruments with tapping and contact modes are available for topographic and phase imaging and roughness measurementsPHI-5000 Versaprobe is equipped with dual Al/Mg anode, focused (10 - 100 µm) and scanned X-ray beam for sample imaging and analysis, hemispherical energy analyzer with multi-channel detection, depth profiling capability Useful for chemical elemental analysis and quantification, Bonding characteristics Operative Modes- Qualitative survey scan, quantitative high resolution scan and depth profiling by simultaneous surface etching scanning.The instrumentation includes the Bruker Optics Hyperion 3000 infrared microscope and Vertex 70 FTIR spectrometer with numerous options for infrared imaging and composition mapping with down to 2-micrometer resolution , in addition to organic functional group analyses.Both transmission and reflection modes available.Micro-Raman/Photoluminescence Spectrometer for non-destructive characterization of materials.Very effective in characterizing carbon materials (CNTs and Diamonds) Complimentary to FT-IR.Measurement of nanomechanical properties such as hardness and Young’s modulus of nanostructured materials and thin films by a nano-tip indentation AMTI Force 5 - An industry standard simulator which can replicate the loading and multi-axis motions associated with joints (Hip, Knee &TMJ)Performs wear simulation of articulation components such as metal-on- metal, diamond-on-metal, metal-on-polymer, and diamond-on-diamondOperated in both force and displacement control modes and allows the continuous or periodic measurement of the forces and moments of the x, y, and z axes under physiological serum conditions Image surface features of metals, biomaterials, thin films, particles, polymers, grain boundaries, composites etc.Energy dispersive X-ray spectroscopy (EDX) to identify elemental composition of materialsCan perform analysis on biological samples using environmental mode (ESEM)Multi-purpose X-ray Diffractometer is non-destructive method to characterize materials’ composition, crystal structure, phase change, grain-size and stress analyses of thin films, polymers and ceramicsCan also perform particle size analysis using small angle X-ray scattering (SAXS)Epitaxial film analysis can be performed using Ultra Fast Reciprocal Space Mapping (URSM)