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Skima FEMTOST Institute December 21 st 2015 Accelerated Lifetime Tests and Failure Analysis of an Electrothermally Actuated MEMS valve firstnamelastnamefemtostfr FEMTOST Institute ID: 830392

tests mems accelerated lifetime mems tests lifetime accelerated air results displacement introduction conclusion motivation membrane µm experimental cycles sem

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Presentation Transcript

Slide1

ICM conference 2015

Haithem

Skima

FEMTO-ST Institute

December 21

st

, 2015

Accelerated Lifetime Tests and Failure Analysis of an Electro-thermally Actuated MEMS valve

firstname.lastname@femto-st.fr

FEMTO-ST Institute,

Besançon

– France

Haithem

Skima

,

Kamal

Medjaher

,

Noureddine

Zerhouni

, Christophe

Varnier

,

Eugen

Dedu

and Julien Bourgeois

Slide2

Outline

H.

Skima

, K.

Medjaher

, N.

Zerhouni

,

C.

Varnier, E. Dedu, J. Bourgeois, ICM Conference, December 20-23,

2015Introduction

Motivation

Accelerated lifetime tests

Results

Conclusion and future work

Slide3

Micro-Electro-Mechanical

Systems: MEMS

A MEMS

is

a micro-system

that integrates

mechanical components using

electricity as source of energy in order to perform measurement functions and / or operating in structure having micrometric dimensions.

Others

MOEMS

RF MEMS

Micro actuators

Micro sensors

Bio MEMS

Categories of MEMS

Applications

Automotive

Aerospace

Biomedical

Optical

Fluidic

Communication technologies

Introduction

Introduction

Motivation Accelerated lifetime tests Results

Conclusion

Slide4

Introduction

Mechanical, electrical and material based failures mechanisms

Failure mechanisms related to manufacturing or to utilization

Mechanical

Electrical

Material

Delamination, Fracture, Fatigue, Creep, Stiction, Plastic-deformation, Adhesion

Degradation of dielectrics, Electrostatic discharge ESD

Electro-migration, Electrical short Circuit, Electrical

stiction

Stiction,

Contamination

Related to utilization

Related to manufacturing

Stiction, Delamination, Fatigue, Creep,

Fracture, Adhesion, ESD,

Electro-migration,

Electrical

short circuit

Stiction, Contamination, Fracture,

Electrical

short circuit

Influence factors

:

temperature, humidity, vibration, noise, dust,

shocks

,

overcharges

[

H. R.

Shea

2007

,

M. McMahon et al. 2012

,

J. Ruan et al. 2009

, R.

Mûller-Fiedler

et al. 2002]

[

M. MATMAT 2010

]

Introduction

Motivation Accelerated lifetime tests Results

Conclusion

Slide5

Introduction

Stiction in electro-thermal actuator

[

M.

Dardalhon

2003

]

Micro-actuator finger fracture

[ B.

Charlot

2001]

Contamination in a comb-drive

[Tanner et al. 2000

]

Stiction

of the finger on the substrate

[Tanner et al. 2000]

Examples of failure mechanisms in MEMS

Introduction

Motivation Accelerated lifetime tests Results

Conclusion

Slide6

Prognostics & Health Management: PHM

Motivation

MEMS

Reliability issues

L

oss of performance

Faults

(Non achieved functions)

Risk of accidents

 Reliability

 Availability

 Security

 cost

Introduction

Motivation

Accelerated lifetime tests Results

Conclusion

Accelerated lifetime tests performing

Health assessment and state estimation

Time to failure prediction

Decision making

Degradation model definition

MEMS

Slide7

Accelerated lifetime tests

Definition

Accelerated lifetime test is an aging of a product that induces normal failures in a short amount of time by applying stress levels much higher than normal ones (stress, strain, temperatures, voltage, vibration rate, pressure, etc.).

The main interest is to observe the evolution over time to predict the life

span.

Reliability results can then be obtained by analyzing the product’s response to such tests.

Difficulty in MEMS failure

analysis

Structures of interest are not exposed for direct observation

Structures that provide the stimulus for motion or actuation are obscured from view

Introduction

Motivation Accelerated lifetime tests

Results Conclusion

Slide8

Accelerated lifetime tests

System description

Electrothermally

actuated MEMS valve designed by

DunAn

Microstaq

company to control flow rates or pressure with high precision at ultra-fast time response (<< 100

ms

). It is currently being used in a number of applications in air conditioning and refrigeration, hydraulic control and air pressure control

Electrical connections

Movable membrane

Fluid connection ports

Common port

Normally closed

Normally open

Normally open

Common port

Normally closed

Scanning Electron Microscope (SEM) pictures (FEMTO-ST)

Anchorage

Anchorage

ᶿ

l

Hot arms

Shuttle

Direction of movement

Maximum actuation voltage: 12V

Current consumption can reach 1A

Introduction

Motivation

Accelerated lifetime tests

Results

Conclusion

Slide9

Computer

Arduino

Voltage suppliers

NI card

Camera

Light source

MEMS

Experimental platform - (FEMTO-ST

)

Accelerated lifetime tests

Experimental setup

PT100 RTD

Input and output of air

Metal plate

Electronic card

MEMS

Pins

Support

1- Experimental platform

Introduction

Motivation

Accelerated lifetime tests

Results

Conclusion

2

- Setup in the SEM

Slide10

Accelerated lifetime tests

NI card

Camera

Arduino card

Voltage supplier

Light source

Pressure regulator

Air filter

MEMS

PT100

Air supply

Temperature measurement

Supply

Image acquisition

Air flow

Electronic card

Global synoptic of the experimental platform

Processing and storage of data

Experimental setup

Introduction

Motivation

Accelerated lifetime tests

Results

Conclusion

1- Experimental platform

Slide11

Accelerated lifetime tests

Direction of motion

Movable Membrane

Direction of motion

Guppy Pro F-031

with

100

fps

Matlab Image-

processing

algorithm

Time

response

parameters

identification

MEMS are supplied with a square signal of

8V

magnitude and a frequency equal to 1Hz.

This voltage is not too high to not bring up prematurely degradation and not to low to obtain enough displacement

The current consumption of a new MEMS at 8V is about 0.55A and the displacement is about 65µm

Introduction

Motivation

Accelerated lifetime tests

Results

Conclusion

Slide12

Accelerated lifetime tests

Movable membrane

Experimental setup

Introduction

Motivation

Accelerated lifetime tests

Results

Conclusion

2

- Setup in the SEM

Electrical connections

MEMS

Slide13

Accelerated lifetime tests

Tests

Tests consist in cycling MEMS valves and changing at each time the operating condition:

Unfiltered air – Experimental platform

Without air – in the SEM

Filtered air – Experimental platform

Unfiltered air

Without air

Filtered air

Cycling four MEMS valves with an unfiltered air

Experiments remained running for more than one month

Measurements were collected every day, after 25000 cycles, and at each measurement the displacement of the membrane is calculated.

Cycling one MEMS valve inside the SEM without air

The displacement of the membrane is calculated by using the SEM images.

Cycling four MEMS valves with filtered air

Experiments remained running for more than three months

Measurements were collected after approximately 90000 cycles.

Introduction

Motivation

Accelerated lifetime tests

Results

Conclusion

Slide14

Results

Unfiltered air

SEM image showing contamination at the normally closed fluid port

Image taking by the camera showing a damaged membrane

Video showing the degraded state of the membrane and its small displacement

Test

Initial displacement

Performed cycles

Displacement at the end

of the test

Membrane state

Unfiltered air

65 µm

1 million

10 µm

degraded

Without air

Test

Initial displacement

Performed cycles

Displacement at the end

of the test

Membrane state

Without air

65 µm

800000

50 µm

good

This test has been stopped since we can not use the SEM for long

Introduction

Motivation

Accelerated lifetime tests

Results

Conclusion

Slide15

Good surface state of the membrane

For the

electrothermally

actuators, a failure is defined as the point at which the displacement decreases by 20%

[Conant et al 1998]

Results

F

iltered air

8 million cycles (guaranteed by the manufacturer) performed without a significant decrease of the displacement (less than 10% of displacement decrease) or membrane degradation

Faulty MEMS

Degradation at the actuator

New MEMS

MEMS at the end cycling

Introduction

Motivation

Accelerated lifetime tests

Results

Conclusion

After 12 million cycles, the displacement is about 15 µm (23% of the initial displacement)

Slide16

Results

Test

Initial displacement

Performed cycles

Displacement at the end

of the test

Membrane state

Unfiltered air

65 µm

1 million

10 µm

degraded

Without air65 µm

800000

50 µmgood

filtered air65 µm

12

million

15 µm

good

The variation of the displacement depends on the degradation

Introduction

Motivation

Accelerated lifetime tests

Results

Conclusion

0

2

4

6

8

10

12

0

50

100

150

MEMS-1

Voltage (V)

Displacement (µm)

MEMS-1 EOL

MEMS-1 cycle0

0

2

4

6

8

10

12

0

20

40

60

80

MEMS-2

Voltage (V)

Displacement (µm)

MEMS-2 EOL

MEMS-2 cycle0

Slide17

Conclusion

Two experimental setup designed to perform accelerated lifetime tests to an electro-thermally actuated MEMS valve

Three accelerated lifetime tests performed

Unfiltered air can cause the contamination at the actuator and the membrane, early failure

Very small displacement of the membrane after 12 million cycles with good surface state

degradation at the actuator which is obscured from view

Perform

new tests by changing input

parameters such as supply

voltage and operating

frequency to

see their impact on the MEMS

degradationAnalyze data collected during tests in order to define a degradation model of the MEMS

Implement Prognostics and Health Management approach to estimate MEMS health states and predict their time to failure

Conclusion

Future works

Introduction

Motivation

Accelerated lifetime tests Results

Conclusion

Slide18

Thank you for your attention

H.

Skima

, K.

Medjaher

, N.

Zerhouni

,

C.

Varnier

, E.

Dedu

, J. Bourgeois,

ICM Conference, December 20-23,

2015